Unistat 930w controlling exothermic reactions in a 100 litre Diehm glass reactor

Effective temperature control of a reaction mass depends on the speed at which the reactor’s jacket temperature can be changed to generate the required Delta-T. This case study demonstrates this perfectly with a Huber Unistat 930w (https://lnkd.in/g-FVR4Q) controlling simulated exothermic reactions in a 100-litre reactor.

In the second reaction of 2kW (1,720kcal/hr), the jacket is cooled from 0°C to -65°C in 10-minutes to bring the rising process temperature rapidly back to the set-point. As the critical process temperature is brought back to the set-point the Delta –T is reduced and then maintained to hold the “reaction” exactly on the set-point.

The full case study can be found here: https://lnkd.in/gFT6mnp and further case studies on the Unistat 930w here: https://lnkd.in/g-Tst_Z